UPLC Fingerprints of Periplaneta americana Extract CⅡ-3

Journal of Dali University ›› 2019, Vol. 4 ›› Issue (2): 27-.

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UPLC Fingerprints of Periplaneta americana Extract CⅡ-3

Zhou Jiaojiao, Zhang Chenggui, Liu Yuyu, Li Ruoshi, Liu Guangming, Xia Conglong

（1.College of Pharmacy and Chemistry, Dali University, Dali, Yunnan 671000, China; 2.Yunnan Provincial Key Laboratory of
Entomological Biopharmaceutical R＆D, Dali, Yunnan 671000, China）

Received:2018-10-03 Revised:2018-10-24 Online:2019-02-15 Published:2019-02-15

Abstract

Abstract:

〔Abstract〕Objective: To establish UPLC fingerprints of Periplaneta americana to assess the quality of different batchs of CⅡ-3
samples. Methods: The analysis of Periplaneta americana extract CⅡ-3 was performed in Phenomenex Gemini 5u C18 110A column
（250 mm × 4.6 mm）and the column temperature was 28 ℃. And acetonitrile-water（0.1% formic acid）was the mobile phase of
gradient elution, set at 214 nm wavelength. The quality of C Ⅱ- 3 was assessed according to the similarity evaluation and the
chemometrics method. Results: The UPLC fingerprints of 12 batches of CⅡ-3 were established. There were 21 common peaks and
fingerprints similarity of 11 batches samples was greater than 0.900. Conclusion: It is the first time that the UPLC fingerprint of CⅡ-3
has been established, which provides a scientific basis for the quality control of Periplaneta americana extract CⅡ-3.

Key words: 〔Key words〕Periplaneta americana L., CⅡ-3, fingerprints, similarity

Zhou Jiaojiao, Zhang Chenggui, Liu Yuyu, Li Ruoshi, Liu Guangming, Xia Conglong. UPLC Fingerprints of Periplaneta americana Extract CⅡ-3[J]. Journal of Dali University, 2019, 4(2): 27-.

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UPLC Fingerprints of Periplaneta americana Extract CⅡ-3

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