含水富有机质页岩重复升温热激增渗实验

doi:10.11885/j.issn.1674-5086.2019.09.17.03

西南石油大学学报(自然科学版) ›› 2021, Vol. 43 ›› Issue (1): 120-132.DOI: 10.11885/j.issn.1674-5086.2019.09.17.03

含水富有机质页岩重复升温热激增渗实验

游利军, 李鑫磊, 康毅力, 陈明君, 郝志伟

油气藏地质及开发工程国家重点实验室·西南石油大学, 四川成都 610500

收稿日期:2019-09-17 出版日期:2021-02-10 发布日期:2021-01-23
通讯作者: 游利军,E-mail:youlj0379@126.com
作者简介:游利军,1976年生,男,汉族,河南洛阳人,教授,博士生导师,主要从事储层保护、非常规油气、岩石物理方面的教学和科研工作。E-mail:youlj0379@126.com
李鑫磊,1996年生,男,汉族,陕西西安人,硕士研究生,主要从事储层保护、非常规天然气和页岩高温热处理等方向研究。E-mail:swpulxl@foxmail.com
康毅力,1964年生,男,汉族,天津蓟县人,教授,博士生导师,主要从事储层保护理论与技术、非常规天然气和油气田开发地质方向科研与教学。E-mail:cwctkyl@163.com
陈明君,1988年生,男,汉族,重庆荣昌人,讲师,博士,主要从事储层保护、非常规气藏多尺度输运、高温高压岩石热物理等方面的工作。E-mail:chenmj1026@163.com
郝志伟,1989年生,男,汉族,河北邢台人,博士研究生,主要从事储层保护、非常规天然气和高温高压岩石热物理等方面的研究。E-mail:swpuhzw@foxmail.com
基金资助:
国家自然科学基金（51674209）；非常规油气层保护四川省青年科技创新团队项目（2016TD0016）；中国博士后科学基金（2017M623062）

An Experimental Study on Cyclical Thermal Stimulation to Enhance Permeability of Water-bearing Organic-rich Shale

YOU Lijun, LI Xinlei, KANG Yili, CHEN Mingjun, HAO Zhiwei

State Key Laboratory of Oil&Gas Reservoir Geology and Exploitation, Southwest Petroleum University, Chengdu, Sichuan 610500, China

Received:2019-09-17 Online:2021-02-10 Published:2021-01-23

摘要/Abstract

摘要： 水力压裂可提高页岩气井产量，但改造尺度多集中于毫米级裂缝，难以沟通微纳孔隙和天然微裂缝，且压后大量压裂液滞留易形成水相圈闭损害，阻碍气体多尺度传输。选取四川盆地下志留统龙马溪组富有机质页岩，模拟水力压裂后页岩储层热处理，开展了加热速率为5 ℃/min干燥页岩重复升温与加热速率为10 ℃/min含水页岩重复升温热激实验，监测了富有机质页岩加热过程中颜色、质量、渗流能力和纵横波速率。研究表明，加热过程中富有机质页岩表观颜色变浅；干燥页岩在600～700 ℃渗透率改善较为明显，渗透率增加了3～5倍；含水页岩渗透率在加热至200～300 ℃时显著提高，纵横波速率整体呈降低的趋势，降低幅度比干燥页岩更大。水岩相互作用、热蒸气压和加热速率引发的空间应力是降低含水页岩热致裂增渗阈值温度的有利条件。

关键词: 富有机质页岩, 气体渗透率, 热激, 增渗, 阈值温度

Abstract: Hydraulic fracturing can improve the production of shale gas wells, but its modification scale is mostly concentrated in millimeter-scale cracks. It is difficult to connect micro-nanopores and natural cracks, and a large number of fracturing fluids remained in formation tend to form water phase trapping damage. Organic-rich shale of the lower silurian Longmaxi formation in the Sichuan Basin was selected to simulate heat treatment of shale gas reservoir after hydraulic fracturing. Heating experiments on dry shales with the heating rate of 5℃/min and water-bearing shale with 10℃/min were carried out to monitor parameters such as color change, mass loss, seepage capacity, and wave velocity. Results have shown that color of organic-rich shale turns lighter when temperature rises. Gas permeability increases 3～5 times when dry shales are heated at 600～700℃. Permeability of water-bearing shale improves more significantly after heating at 200～300℃. Wave velocity decreases more after water-bearing shale heating than that of dry shales. Water-rock interaction, hot vapor pressure and spatial thermal stress change induced by heating rate are favorable conditions for reducing threshold temperature of shale.

Key words: organic-rich shale, gas permeability, thermal stimulation, permeability improvement, threshold temperature

中图分类号:

TE377

游利军, 李鑫磊, 康毅力, 陈明君, 郝志伟. 含水富有机质页岩重复升温热激增渗实验[J]. 西南石油大学学报(自然科学版), 2021, 43(1): 120-132.

YOU Lijun, LI Xinlei, KANG Yili, CHEN Mingjun, HAO Zhiwei. An Experimental Study on Cyclical Thermal Stimulation to Enhance Permeability of Water-bearing Organic-rich Shale[J]. Journal of Southwest Petroleum University(Science & Technology Edition), 2021, 43(1): 120-132.

0
/ / 推荐

导出引用管理器 EndNote|Ris|BibTeX

链接本文: http://journal15.magtechjournal.com/Jwk_xnzk/CN/10.11885/j.issn.1674-5086.2019.09.17.03

http://journal15.magtechjournal.com/Jwk_xnzk/CN/Y2021/V43/I1/120

参考文献

[1] 唐颖,张金川,张琴,等. 页岩气井水力压裂技术及其应用分析[J]. 天然气工业, 2010, 30(10):33-38. doi:10.3787/j.issn.1000-0976.2010.10.008 TANG Ying, ZHANG Jinchuan, ZHANG Qin, et al. An analysis of hydraulic fracturing technology in shale gas wells and its application[J]. Natural Gas Industry, 2010, 30(10):33-38. doi:10.3787/j.issn.1000-0976.2010.10.008
[2] 贾长贵,路保平,蒋廷学,等. DY2HF深层页岩气水平井分段压裂技术[J]. 石油钻探技术, 2014, 42(2):85-90. doi:10.3969/j.issn.10010890.2014.02.017 JIA Changgui, LU Baoping, JIANG Tingxue, et al. Multi-stage horizontal well fracturing technology in deep shale gas Well DY2 HF[J]. Petroleum Drilling Techniques, 2014, 42(2):85-90. doi:10.3969/j.issn.10010890.2014.02.017
[3] 张东晓,杨婷云. 美国页岩气水力压裂开发对环境的影响[J]. 石油勘探与开发, 2015, 42(6):801-807. doi:10.11698/PED.2015.06.14 ZHANG Dongxiao, YANG Tingyun. Environmental impacts of hydraulic fracturing in shale gas development in the United States[J]. Petroleum Exploration and Development, 2015, 42(6):801-807. doi:10.11698/PED.2015.06.14
[4] 叶登胜,尹丛彬,蒋海,等. 四川盆地南部页岩气藏大型水力压裂作业先导性试验[J]. 天然气工业,2011,31(4):48-50. doi:10.3787/j.issn.1000-0976.2011.04.011 YE Dengsheng, YIN Congbin, JIANG Hai, et al. A pilot test of large-scale hydraulic fracturing in shale gas reservoir of the southern Sichuan Basin[J]. Natural Gas Industry, 2011, 31(4):48-50. doi:10.3787/j.issn.1000-0976.2011.04.011
[5] 张建,熊炜,赵宇新. 隆页1HF井桥塞分段大型压裂技术[J]. 油气藏评价与开发, 2018, 8(1):76-80. ZHANG Jian, XIONG Wei, ZHAO Yuxin. Large segment fracturing technology of pumping bridge plug in Well Longye-lHF[J]. Reservoir Evaluation and Development, 2018, 8(1):76-80.
[6] 方朝合,黄志龙,王巧智,等. 页岩气藏超低含水饱和度形成模拟及其意义[J]. 地球化学, 2015, 44(3):267-274. doi:10.3969/j.issn.0379-1726.2015.03.006 FANG Chaohe, HUANG Zhilong, WANG Qiaozhi, et al. Simulation of utlra-low water saturation in shale gas reservoirs and its significance[J]. Geochimica, 2015, 44(3):267-274. doi:10.3969/j.issn.0379-1726.2015.03.006
[7] XU Chengyuan, KANG Yili, YOU Zhenjiang, et al. Review on formation damage mechanisms and processes in shale gas reservoir:Known and to be known[J]. Journal of Natural Gas Science and Engineering, 2016, 36:1208-1219. doi:10.1016/j.jngse.2016.03.096
[8] 康毅力,张晓怡,游利军,等. 页岩气藏自然返排缓解水相圈闭损害实验研究[J]. 天然气地球科学, 2017, 28(6):819-827. doi:10.11764/j.issn.1672-1926.2017.05.009 KANG Yili, ZHANG Xiaoyi, YOU Lijun, et al. The experimental research on spontaneous flowback relieving aqueous phase trapping damage in shale gas reservoirs[J]. Natural Gas Geoscience, 2017, 28(6):819-827. doi:10.11764/j.issn.1672-1926.2017.05.009
[9] 陈明君,康毅力,游利军. 利用高温热处理提高致密储层渗透性[J]. 天然气地球科学, 2013, 24(6):1226-1231. CHEN Mingjun, KANG Yili, YOU Lijun. Advantages in formation heat treatment to enhance permeability in tight reservoir[J]. Natural Gas Geoscience, 2013, 24(6):1226-1231.
[10] 游利军,康毅力,陈强,等. 氧化爆裂提高页岩气采收率的前景[J]. 天然气工业, 2017, 37(5):53-61. doi:10.3787/j.issn.1000-0976.2017.05.007 YOU Lijun, KANG Yili, CHEN Qiang, et al. Prospect of shale gas recovery enhancement by oxidation-induced rock burst[J]. Natural Gas Industry, 2017, 37(5):53-61. doi:10.3787/j.issn.1000-0976.2017.05.007
[11] KANG Yili, CHEN Mingjun, CHEN Zhangxin, et al. Investigation of formation heat treatment to enhance the multiscale gas transport ability of shale[J]. Journal of Natural Gas Science and Engineering, 2016, 35:265-275. doi:10.1016/j.jngse.2016.08.058
[12] 游利军,李鑫磊,康毅力,等. 富有机质页岩储层热激致裂增渗的有利条件[J]. 天然气地球科学, 2020, 31(3):325-334. doi:10.11764/j.issn.1672-1926.2019.11.009 YOU Lijun, LI Xinlei, KANG Yili, et al. Advantages of thermal stimulation to induce shale cracking after hydraulic fracturing over organic-rich shale reservoirs[J]. Natural Gas Geoscience, 2020, 31(3):325-334. doi:10.11764/j.issn.1672-1926.2019.11.009
[13] JAMALUDDIN A K M, VANDAMME L M, MANN B K. Formation heat treatment (FHT):A state-of-the art technology for near-wellbore formation damage treatment[C]. SPE PETSOC-95-67, 1995. doi:10.2118/95-67
[14] 李皋,孟英峰,董兆雄,等. 砂岩储集层微波加热产生微裂缝的机理及意义[J]. 石油勘探与开发, 2007, 34(1):93-97. doi:10.3321/j.issn:1000-0747.2007.01.018 LI Gao, MENG Yingfeng, DONG Zhaoxiong, et al. Mechanisms and significance of microfractures generated by microwave heating in sandstone reservoirs[J]. Petroleum Exploration and Development, 2007, 34(1):93-97. doi:10.3321/j.issn:1000-0747.2007.01.018
[15] JAMALUDDIN A K M, VANDAMME L M, NAZARKO T W, et al. Heat treatment for clay-related near wellbore formation damage[J]. Journal of Canadian Petroleum Technology, 1998, 37(1):56-63. doi:10.2118/98-01-09
[16] LIU Junrong, LI Boyu, TIAN Wei, et al. Investigating and predicting permeability variation in thermally cracked dry rocks[J]. International Journal of Rock Mechanics and Mining Sciences, 2018, 103:77-88. doi:10.1016/j.ijrmms.2018.01.023
[17] CHA Minsu, ALQAHTANI N B, YIN Xiaolong, et al. Laboratory system for studying cryogenic thermal rock fracturing for well stimulation[J]. Journal of Petroleum Science and Engineering, 2017, 156:780-789. doi:10.1016/j.petrol.2017.06.062
[18] SUNDBERG J, BACK P, CHRISTIANSSON R, et al. Modelling of thermal rock mass properties at the potential sites of a Swedish nuclear waste repository[J]. International Journal of Rock Mechanics and Mining Sciences, 2009, 46(6):1042-1054. doi:10.1016/j.ijrmms.2009.02.004
[19] BRUEL D. Impact of induced thermal stresses during circulation tests in an engineered fractured geothermal reservoir:Example of the soultz-sous-forêts european hot fractured rock geothermal project, Rhine Graben, France[J]. Oil & Gas Science and Technology-Revue, IFP, 2002, 57(5):459-470. doi:10.2516/ogst:2002030
[20] 付亚荣,李明磊,王树义,等. 干热岩勘探开发现状及前景[J]. 石油钻采工艺, 2018, 40(4):526-540. doi:10.13639/j.odpt.2018.04.022 FU Yarong, LI Minglei, WANG Shuyi, et al. Present situation and prospect of hot dry rock exploration and development[J]. Oil Drilling & Production Technology, 2018, 40(4):526-540. doi:10.13639/j.odpt.2018.04.022
[21] FOWLER T D, VINEGAR H J. Oil shale ICP-Colorado Field pilots[C]. SPE 121164-MS, 2009. doi:10.2118/121164-MS
[22] 汪友平,王益维,孟祥龙,等. 流体加热方式原位开采油页岩新思路[J]. 石油钻采工艺, 2014, 36(4):71-74. doi:10.13639/j.odpt.2014.04.018 WANG Youping, WANG Yiwei, MENG Xianglong, et al. A new idea for in-situ retorting oil shale by way of fluid heating technology[J]. Oil Drilling & Production Technology, 2014, 36(4):71-74. doi:10.13639/j.odpt.2014.04.018
[23] ZOU Caineng, CHEN Yanpeng, KONG Lingfeng, et al. Underground coal gasification and its strategic significance to the development of natural gas industry in China[J]. Petroleum Exploration and Development, 2019, 46(2):205-215. doi:10.1016/S1876-3804(19)60002-9
[24] BHUTTO A W, BAZMI A A, ZAHEDI G. Underground coal gasification:From fundamentals to applications[J]. Progress in Energy and Combustion Science, 2013, 39(1):189-214. doi:10.1016/j.pecs.2012.09.004
[25] SHAHTALEBI A, KHAN C, DMYTERKO A, et al. Investigation of thermal stimulation of coal seam gas fields for accelerated gas recovery[J]. Fuel, 2016, 180:301-313. doi:10.1016/j.fuel.2016.03.057
[26] WANG Hongcai, REZAEE R, SAEEDI A. Evaluation of microwave heating on fluid invasion and phase trapping in tight gas reservoirs[C]. SPE 176906-MS, 2015. doi:10.2118/176906-MS
[27] WANG Hanyi, AJAO O, ECONOMIDES M J. Conceptual study of thermal stimulation in shale gas formations[J]. Journal of Natural Gas Science and Engineering, 2014, 21:874-885. doi:10.1016/j.jngse.2014.10.015
[28] HAYATDAVOUDI A, NIZAMUTDINOV R, KRAVETS J, et al. Increasing the pierre shale reservoir volume using heat:Part I[C]. ARMA-2015-816, 2015.
[29] 杨天鸿,唐春安,徐涛. 岩石破裂过程的渗流特性——理论、模型与应用[M]. 北京:科学出版社,2004. YANG Tianhong, TANG Chun'an, XU Tao. Seepage characteristic in rock failure:Theory model and applications[M]. Beijing:Science Press, 2004.
[30] 游利军,程秋洋,康毅力,等. 页岩裂缝网络水相自吸试验[J]. 中国石油大学学报(自然科学版), 2018, 42(1):82-89. doi:10.3969/j.issn.1673-5005.2018.01.010 YOU Lijun, CHENG Qiuyang, KANG Yili, et al. Experimental study on spontaneous water imbibition in fracture networks of shale rocks[J]. Journal of China University of Petroleum (Edition of Natural Science), 2018, 42(1):82-89. doi:10.3969/j.issn.1673-5005.2018.01.010
[31] HETTEMA M H H, WOLF K H A A, Pater C J. The influence of steam pressure on thermal spalling of sedimentary rock:Theory and experiments[J]. International Journal of Rock Mechanics & Mining Sciences, 1998, 35(1):3-15. doi:10.1016/S0148-9062(97)00318-5
[32] HAYATDAVOUDI A, CHITILA D, BOUKADI F. Effect of cyclic temperature, water vapor and exposure time on micro fracture propagation in shale[C]. ISRM-13CONGRESS-2015-364, 2015.
[33] CHEN Jinhong, GEORGI Daniel, LIU Huihai, et al. Fracturing tight rocks by elevated pore water pressure using microwaving and its applications[C]. SPWLA-2015-RRR, 2015.
[34] KEANEY G M, JONES C, MEREDITH P, et al. Thermal damage and the evolution of crack connectivity and permeability in ultra-low permeability rocks[C]. ARMA-04-537, 2004.
[35] KIM K M, KEMENY J. Effect of thermal shock and rapid unloading on mechanical rock properties[C]. ARMA-09-084, 2009.
[36] YIN Tubing, SHU Ronghua, LI Xibing, et al. Comparison of mechanical properties in high temperature and thermal treatment granite[J]. Transactions of Nonferrous Metals Society of China, 2016, 26(7):1926-1937. doi:10.1016/S1003-6326(16)64311-X
[37] ZHU Tantan, JING Hongwen, SU Haijian, et al. Physical and mechanical properties of sandstone containing a single fissure after exposure to high temperatures[J]. International Journal of Mining Science and Technology, 2016, 26(2):319-325. doi:10.1016/j.ijmst.2015.12.019
[38] KANG Yili, CHEN Mingjun, YOU Lijun, et al. Laboratory measurement and interpretation of the changes of physical properties after heat treatment tight porous media[J]. Journal of Chemistry, 2015:1-10. doi:10.1155/2015/341616
[39] LIU Shi, XU Jinyu. An experimental study on the physicomechanical properties of two post-high-temperature rocks[J]. Engineering Geology, 2015, 185:63-70. doi:10.1016/j.enggeo.2014.11.013
[40] SUN Qiang, ZHANG Weiqiang, XUE Lei, et al. Thermal damage pattern and thresholds of granite[J]. Environmental Earth Sciences, 2015, 74(3):2341-2349. doi:10.1007/s12665-015-4234-9

含水富有机质页岩重复升温热激增渗实验

An Experimental Study on Cyclical Thermal Stimulation to Enhance Permeability of Water-bearing Organic-rich Shale

RichHTML

PDF (PC)

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 3

编辑推荐

Metrics

本文评价

[1]	游利军, 徐洁明, 康毅力, 程秋洋, 周洋. 考虑氧化作用的富有机质页岩吸附水量[J]. 西南石油大学学报(自然科学版), 2019, 41(6): 106-116.
[2]	康建威, 余谦, 闫剑飞, 孙媛媛, 戚明辉. 渝南-黔北五峰组-龙马溪组页岩气地质特征[J]. 西南石油大学学报(自然科学版), 2016, 38(6): 49-60.
[3]	陈二丁陈大钧李宾元. 高渗透水泥施工及防砂性能研究 [J]. 西南石油大学学报(自然科学版), 2001, 23(2): 47-49.