西南石油大学学报(自然科学版) ›› 2012, Vol. 34 ›› Issue (5): 153-158.

• 油气化学工程与化工 • Previous Articles     Next Articles

Study of Metal-phthalocyanine Encapsulated in Mesoporous MolecularSieves MCM-41

Cui Zixiang1, Xue Yongqiang1, Li Ping2   

  1. 1. College of Chemistry and Chemical Engineering；Taiyuan University of Technology，Taiyuan，Shanxi 030024，China2. Search Center of Environmental Science and Engineering，Shanxi University，Taiyuan，Shanxi 030006，China
  • Received:1900-01-01 Revised:1900-01-01 Online:2012-10-01 Published:2012-10-01

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Abstract: Zn-phthalocyanine complex（Ⅱ），which periphery has substituents was synthesized，and encapsulated in mesoporous
molecular sieves MCM-41. The prepared samples was characterized by FT-IR，UV-vis-Nir，XRD，FESEM，TEM and
N2 adsorption-desorption instrument. The research shows that the prepared phthalocyanine copper zinc can be encapsulated in
mesoporous molecular sieves MCM-41 in the form of monomer and dipolymer. The prepared phthalocyanine zinc with high
concentration encapsulated in MCM-41 is in favour of preparing mesoporous molecular sieves samples with higher crystallinity
and pore canal order.

Key words: MCM-41, load, phthalocyanine